An industrial MPCVD reactor growing Type IIa Grade-D Single Crystal Diamond on 7 HPHT seeds simultaneously, enabling vertically integrated NV-center quantum sensors for the next generation of breath diagnostics and beyond.
Microwave Plasma Chemical Vapor Deposition reactor engineered for high-yield, repeatable Single Crystal Diamond synthesis under demanding tropical conditions (45 °C, 90 % RH).
Solid-state generator (top-mounted, easy-repair). WR340 waveguide, 3-stub auto-tuner, > 90 % coupling, < 5 % reflected power.
Base pressure < 10⁻⁵ mbar. Operating 30–300 mbar. KF/CF flange combination, FFKM seals, 3+ viewports for OES, pyrometry, camera.
7× HPHT seeds, 20×20 mm. Mo / W water-cooled holder with seed pockets. Per-seed temperature monitoring (multi-channel pyrometry).
H₂ 50 slm (6N), CH₄ 2 slm (5N/6N), N₂ for NV doping, O₂ for etching, Ar purge. Bronkhorst MFCs · EtherCAT · NanoZ leak detection.
Closed-loop, derated for 45 °C ambient. Optional shared absorption-cooling system across 1950 reactors per facility.
3-phase 400 V / 50 Hz (India). UPS for control system ≥ 15 min ride-through. Schaltschrank Rittal AX 1340 IP55.
PROFINET, MQTT, OPC-UA, RS-485. 16–24-bit ADC ≥ 1 Hz. Web HMI (React + FastAPI). InfluxDB + PostgreSQL · Grafana.
Plasma OES (H_α, C₂ Swan, CH). Multi-channel pyrometry 600–1200 °C. Laser interferometry growth-rate. NanoZ MEMS H₂ leak.
A nitrogen-vacancy center is a substitutional N atom adjacent to a lattice vacancy with C₃ᵥ symmetry — the most well-characterised solid-state quantum defect known to physics.
Zero-Field Splitting D = 2.87 GHz at room temperature. Shifts with temperature (−74 kHz/K), pressure, strain, and electric field — making the NV a multi-modal sensor.
Green-laser excitation pumps the spin to |0〉 (~80 % polarization). Microwave-resonant transitions to |±1〉 reduce fluorescence — the basis of ODMR.
A single NV ensemble simultaneously senses magnetic field, temperature, pressure, electric field, and (in the right geometry) biomolecular fingerprints — all in ambient conditions.
Instead of running isolated lab batches for years, we build the master recipe on a data foundation of 10 000–15 000 producing reactors — each running multiple growth batches per year, fed by the fleet of our partner Vallabhbhai Patel in Surat and Mumbai. A digital twin learns the coupling between plasma, gas chemistry and geometry; our in-line metrology then runs the finished recipe in milliseconds on every reactor.
The Surat / Mumbai diamond hub runs hundreds of HPHT and MPCVD reactors today — most of them without in-line diagnostics. We install the identical metrology package into every delivered and every retrofitted reactor: NanoZ MOx array (H₂/CH₄/trace), ThermoAir 5.0 mass-flow, multi-channel pyrometry, plasma OES (H_α/C₂/CH), chamber pressure, substrate T. Every reactor becomes a data sensor — while remaining in full production for the partner.
The Vallabhbhai Patel fleet covers 10 000–15 000 producing reactors across Surat and Mumbai. Every reactor runs multiple growth batches per year, which streams a six-figure count of fully instrumented growth runs per year into the TSR cloud, each at second-level resolution across every sensor, plus gold-standard labels (Raman / XRD / ODMR) at the end of every run. Data residency Switzerland, ISO 27001-grade pipeline. Raw process data stays partner-owned; derived models stay TSR-owned.
A hybrid model combining physics-based MPCVD equations (plasma Boltzmann, gas-phase kinetics, heat balance) with data-driven correction (XGBoost / Gaussian Process / 1D-CNN over time series) represents every reactor as its own digital twin. The model predicts growth rate, crystal quality and — most importantly — the NV center yield from setpoint trajectories, with a confidence interval per run.
With a trained digital twin, recipe optimization runs as Bayesian optimization / reinforcement learning in silico — thousands of virtual runs per hour, instead of one real run per day. Convergence on an NV-optimized master recipe (targeted [N] doping, ¹²C enrichment, vacancy engineering via pressure/power modulation) within an estimated 8–16 weeks — versus the 3–5 years of classical single-lab DoE iteration.
Once the master recipe is locked, it doesn't run as a static table but as a closed-loop trajectory: NanoZ MOx delivers ppb-grade gas composition (T₉₀ < 1 s), ThermoAir 5.0 measures mass flow at 0.5 % accuracy (ms-grade resolution), OES and pyrometry close the plasma/temperature picture. The Beckhoff PLC tick runs at 1 ms, MFC setpoint updates land in under 10 ms. Every drift in the plasma chemistry is corrected before the crystal even sees it — that's what makes the master recipe reproducible from reactor to reactor.
Working meeting — left to right: Jayesh Savalia (Co-Owner, TSR AI NANOZ Sensors Pvt. Ltd.), Vallabhbhai Patel (Owner, Kira / Kiran Diamonds) and Michael Scheller (CEO, TSR Messtechnik AG) at the reception of Kira Diamonds Pvt. Ltd. in Surat. Agenda: retrofit strategy for the existing reactor fleet, the data-sharing model for the digital twin, the scale-up path for SURAT-7B inside the Patel group and the NV-substrate distribution channel through the Kiran Diamonds network in Mumbai.
Owner of Kira Diamonds Pvt. Ltd. (Surat, Gujarat) and Kiran Diamonds (Mumbai, Maharashtra) — one of India's largest vertically integrated diamond houses, covering rough sourcing, HPHT/MPCVD synthesis, cutting, polishing and end-customer distribution under one roof.
SURAT-7B operates in Surat, Gujarat — Make-in-India, DVA ≥ 40 %, PLI scheme eligible. Dramatically lower CapEx and OpEx vs. EU/US competitors.
In-house ppb-level gas monitoring (H₂, CH₄, VOC) and hydrogen-leak detection — only TSR has this vertical capability for MPCVD process control.
Manufacturing partner TSR Messtechnik AG is certified to ISO 9001:2015 + ISO/IEC 17025:2018 across its Swiss and Indian entities, with a Swiss precision-instrumentation tradition going back to 1925 and calibration traceability to its NASA / CERN / Roche / Novartis customer base.
Single Crystal Diamond samples · NV-grade plates · OEM long-term supply agreements · joint research collaborations.
SURAT-7B reactor specs, NV physics, process recipes and the integrated NANOZ-NV control patent.